HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 71197Generated: October 29, 2026
Hydrazine hydrate (1:1) → HCID 66608309, compound
https://huagongshe.com/reaction/71197
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | methyl 4-(4-chloro-1H-imidazol-1-yl)-3-methoxybenzoate | HCID 66608175 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 66608309 | HCID 66608309 | — |
Reaction Steps
To a mixture of methyl 4-(4-chloro-1H-imidazol-1-yl)-3-methoxybenzoate (25.5 mg) in methanol (1 mL) was added hydrazine monohydrate (0.019 mL) at room temperature, the mixture was stirred at 60° C. overnight, and the solvent was evaporated under reduced pressure. The residue was washed with ethyl acetate to give the title compound (12.7 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08822699B2 |
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| Source dataset | uspto-grants-2014_09 |
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| ORD ID | ord-f7d3b1b7445d4dfea80014406585c417 |
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| Source note | uspto-grants-2014_09 |
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