1,4-Dioxane hydrochloride → HCID 66977253, compound

Participants

Reaction Steps

To an ice-cold solution of O1-tert-butyl O4-ethyl 4-methylsulfanylpiperidine-1,4-dicarboxylate (0.23 g, 7.75 mmol) in 1,4-dioxane (20 mL) was added HCl-dioxane (4 M, 15 mL) solution and the mixture stirred at rt for 30 min. After completion of reaction (by TLC), the solvent was evaporated to obtain a brownish solid material (0.17 g) that was carried forward to the next step without further purification. MS: 204.10 [M+H]+.

Provenance & Evidence