HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86729487, compound → HCID 68539279, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86729487 | HCID 86729487 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68539279 | HCID 68539279 | 53.2% |
Reaction Steps
To a solution of 2-benzyloctahydropyrano[3,4-c]pyrrole (0.45 g) in EtOH (30 mL) was added 20% Pd(OH)2 (0.30 g). The suspension was stirred under H2 for 12 h and filtered. The filtrate was concentrated in vacuo to give the title compound (0.14 g). The compound was characterized by the following spectroscopic data: MS (ESI, pos. ion) m/z: 128.3 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181277B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-b58a8a70399d4663bf32285064d66fcd |
| Source note | uspto-grants-2015_11 |