Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 712514Generated: November 1, 2026

HCID 86729513, compound → HCID 86729515, compound

https://huagongshe.com/reaction/712514

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86729513HCID 86729513—
CatalystPalladiumHCID 23938—
SolventTetrahydrofuranHCID 8028—
ProductHCID 86729515HCID 86729515—

Reaction Conditions

Temperature50 °C

Reaction Steps

A mixture of (4aR,7aR)-benzyl tetrahydro-2H-[1,4]dioxino[2,3-c]pyrrole-6(3H)-carboxylate (140.0 mg, 0.53 mmol) and 10% Pd/C (0.56 mg, 0.053 mmol) in THF (6 mL) was stirred for 5.0 h at 50° C. The resulted mixture was filtered. The filtrate was concentrated in vacuo and the residue was used for the next step without further purification.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09181277B2
Source datasetuspto-grants-2015_11
ORD IDord-9d7a31be69cb4c25a0bccc9303d6d576
Source noteuspto-grants-2015_11