HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 712514Generated: November 1, 2026
HCID 86729513, compound → HCID 86729515, compound
https://huagongshe.com/reaction/712514
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 86729513 | HCID 86729513 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86729515 | HCID 86729515 | — |
Reaction Steps
A mixture of (4aR,7aR)-benzyl tetrahydro-2H-[1,4]dioxino[2,3-c]pyrrole-6(3H)-carboxylate (140.0 mg, 0.53 mmol) and 10% Pd/C (0.56 mg, 0.053 mmol) in THF (6 mL) was stirred for 5.0 h at 50° C. The resulted mixture was filtered. The filtrate was concentrated in vacuo and the residue was used for the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09181277B2 |
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| Source dataset | uspto-grants-2015_11 |
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| ORD ID | ord-9d7a31be69cb4c25a0bccc9303d6d576 |
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| Source note | uspto-grants-2015_11 |
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