HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2R)-1-Boc-4-oxopipecolic acid → HCID 117966684, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2R)-1-Boc-4-oxopipecolic acid | HCID 44119498 | — |
| Reactant | (S)-Methyl 4-(1-aminoethyl)benzoate hydrochloride | HCID 57462942 | — |
| Product | HCID 117966684 | HCID 117966684 | — |
Reaction Steps
The title compound (D60) (300 mg) was prepared according to the general procedure for amides preparation (Method C) starting from (R)-1-(tert-butoxycarbonyl)-4-oxopiperidine-2-carboxylic acid (200 mg; available from Aldrich#701130) and (S)-methyl 4-(1-aminoethyl)benzoate hydrochloride (195 mg). Reaction time: 1 h
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181279B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-94da9934035348c2bb8657dec5d572d7 |
| Source note | uspto-grants-2015_11 |