HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrabutylammonium Hydroxide → 1-Butanaminium, N,N,N-tributyl-, methyl carbonate (1:1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Reactant | Methylcarbonate | HCID 4585885 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 1-Butanaminium, N,N,N-tributyl-, methyl carbonate (1:1) | HCID 11141661 | — |
Reaction Steps
As above, 30 g of a 40% b.w. solution of tetrabutylammonium hydroxide (46.0 mmole base) in methanol was mixed with 45 g DMC. After decantation of some precipitate, a clear solution of 0.68 meq methylcarbonate per g solution was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181452B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-17db886c70da4599ae7c771aa8031604 |
| Source note | uspto-grants-2015_11 |