HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67009156, compound → HCID 136627229, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67009156 | HCID 67009156 | — |
| Reactant | 2-(Aminomethyl)-7,8-dihydro-3H-pyrano[4,3-D]pyrimidin-4(5H)-one | HCID 135741894 | — |
| Product | HCID 136627229 | HCID 136627229 | 39.7% |
Reaction Steps
The title compound (1.2 g) was prepared according the general procedure of Example 1 from 2-(4-(methoxycarbonyl)piperidin-1-yl)acetic acid (2.2 g, 11 mmol) and 2-aminomethyl-3,5,7,8-tetrahydro-pyrano[4,3-d]pyrimidin-4-one (1.5 g, 8.3 mmol). MS m/z 365.3 (M+1), retention time=1.46 min.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181266B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-d89ea89eb27241a0a9a20fca18e78e67 |
| Source note | uspto-grants-2015_11 |