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Thionyl Chloride → 4-(Diethylamino)benzoyl chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | Benzoic acid, 4-(diethylamino)- | HCID 79480 | — |
| 溶媒 | Benzene | HCID 241 | — |
| 生成物 | 4-(Diethylamino)benzoyl chloride | HCID 12707021 | 93% |
反応手順
First, thionyl chloride was added dropwise to a benzene solution (20 mL) containing 0.96 g (5 mmol) of 4-(diethylamino)benzoic acid (a compound (10-2) in the following reaction formula) and was allowed to react at room temperature in a nitrogen atmosphere, yielding 4-(diethylamino)benzoic acid chloride (a compound (10-3) in the following reaction formula, 4.65 mmol, yield 93%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09182632B2 |
| 出典データセット | uspto-grants-2015_11 |
| ORD ID | ord-0e7ec860f1834fab876f9a62ca64ef3e |
| 出典メモ | uspto-grants-2015_11 |