HuagongsheHuagongshe Chemistry Print Report · For research reference only
Toluene → HCID 58225146, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 58225130 | HCID 58225130 | — |
| Product | HCID 58225146 | HCID 58225146 | — |
Reaction Steps
(1,2-dihydrocyclobutabenzen-4-yl)diphenylmethanol (0.8 g, 2.8 mmol) and acetylchloride (20 ml, 280 mmol) was refluxed in 30 mL of toluene for 2 hours. The solvent was then evaporated under reduced pressure. The residue was used for the next step without purification. 0.8 g of the product was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09184394B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-73f3bbb39331443bb1423d0afd61d086 |
| Source note | uspto-grants-2015_11 |