HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67972043, compound → HCID 66692371, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67972043 | HCID 67972043 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 66692371 | HCID 66692371 | — |
Reaction Steps
The title compound from Step A above (2.6 g, 12.2 mmol) was dissolved in 4 M HCl in dioxane (200 mL) and stirred at RT overnight. The product was concentrated under reduced pressure and dried under high vacuum to give 6-(1H-tetrazol-1-yl)-3-azabicyclo[3.1.0]hexane. ESI-MS calculated for C6H9N5: Exact Mass: 151.09. Found 152.05.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09186354B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-ad0b47ab09d1410b9fa56903969b1d1a |
| Source note | uspto-grants-2015_11 |