反应详情

The title compound from Step A above (2.6 g, 12.2 mmol) was dissolved in 4 M HCl in dioxane (200 mL) and stirred at RT overnight. The product was concentrated under reduced pressure and dried under high vacuum to give 6-(1H-tetrazol-1-yl)-3-azabicyclo[3.1.0]hexane. ESI-MS calculated for C6H9N5: Exact Mass: 151.09. Found 152.05.

1. concentrationThe product was concentrated under reduced pressure
2. customdried under high vacuum