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HRID713773

反应详情

EQUATION

反应方程式

HRID 713773 的结构方程式

REACTANTS

反应物

3
结构：N
HCID222

Ammonia gas

H3N

结构：NC(=NO)c1cccnc1
HCID308113

N-Hydroxynicotinimidamide

C6H7N3O

结构：O=C(O)c1cc(F)c(F)c(O)c1F
HCID2734270

3-Hydroxy-2,4,5-trifluorobenzoic acid

C7H3F3O3

PRODUCTS

生成物

1
结构：Oc1c(F)c(F)cc(-c2nc(-c3cccnc3)no2)c1F
HCID86621256

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the procedure of Example 8 using N′-hydroxynicotinimidamide (Aldrich) and 2,4,5-trifluoro-3-hydroxybenzoic acid (Aldrich). 1H NMR (300 MHz, CD3OD) δ 7.63-7.76 (m, 2H), 8.44 (dt, J=7.9, 2.0 Hz, 1H), 8.83 (dd, J=4.8, 1.6 Hz, 1H), 9.25 (d, J=1.6 Hz, 1H) ppm; MS (DCl/NH3) m/z 294 (M+H)+.