反应详情

Bromovaleric acid (2 g) was dissolved in aqueous solution of dimethylamine and stirred at room temperature overnight. The solvent was removed on a rotovap and the residue treated with an aqueous solution containing one equivalent of sodium bicarbonate. The solvent was removed, the residue suspended in ethanol and filtered. The solvent was removed from the filtrate and the residue suspended in methylene chloride and suspended again. After filtration, removal of the solvent from the filtrate yielded an oil (1.3 g) that slowly crystallized on storage.

1. customThe solvent was removed on a rotovap
2. additionthe residue treated with an aqueous solution
3. customThe solvent was removed
4. filtrationfiltered
5. customThe solvent was removed from the filtrate
6. filtrationAfter filtration, removal of the solvent from the filtrate