HuagongsheHuagongshe Chemistry Print Report · For research reference only
(4-Fluoro-3-methylphenyl)boronic acid → HCID 71811645, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (4-Fluoro-3-methylphenyl)boronic acid | HCID 2774580 | — |
| Reactant | N-(4-Bromo-6,7-dihydro-5H-cyclopenta[c]pyridin-7-yl)propionamide | HCID 86685956 | — |
| Product | HCID 71811645 | HCID 71811645 | 86% |
Reaction Steps
In analogy to the procedure described for the preparation of example 1, (rac)-N-(4-bromo-6,7-dihydro-5H-cyclopenta[c]pyridin-7-yl)propionamide (intermediate A-4) was reacted with 4-fluoro-3-methylphenylboronic acid to give the title compound as grey solid in 86% yield. MS: 299.2 (M+H+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187429B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-be60839dab9542819b0f4fa9e691f7c9 |
| Source note | uspto-grants-2015_11 |