Hydrochloric Acid → HCID 178510370, compound

Participants

Reaction Conditions

Reaction Steps

0.1 g (0.268 mmol) of 4-[4-(2-hydroxyethoxy)phenyl]-2-(phenylthio)pyridine-3,5-dicarbonitrile (Example 47A) was initially charged in 1 ml of DMF. 73 mg (0.937 mmol) of sodium sulfide were added, and the mixture was then stirred at 80° C. for 2 h and stirred further at RT overnight. 20 ml of 1N hydrochloric acid were added, and the residue was filtered off and washed thoroughly with water.

Provenance & Evidence