HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 145883-50-7
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-Aminobenzyl alcohol | HCID 80293 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 145883-50-7 | HCID 66630476 | — |
Reaction Steps
At 0° C., 2.0 g (16.24 mmol) of 3-aminobenzyl alcohol were initially charged in 60 ml of dichloromethane. 5.8 g (48.72 mmol) of thionyl chloride were added dropwise, and the reaction solution was stirred at RT overnight. The reaction solution was evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187428B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-d0c4d0c29c62452290d09987c625dc40 |
| Source note | uspto-grants-2015_11 |