HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorophenylboronic acid → HCID 69940682, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorophenylboronic acid | HCID 2734322 | — |
| Reactant | HCID 69939744 | HCID 69939744 | — |
| Product | HCID 69940682 | HCID 69940682 | — |
Reaction Steps
Analogously to the preparation of Example 122, 265 mg (0.50 mmol) of the compound from Example 104A were reacted with 194 mg (0.74 mmol) of 2-chlorophenylboronic acid. This gave 54 mg (19% of theory) of the target compound of a purity of 98% and 167 mg (49% of theory) of a purity of 83%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187466B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-ad83559188a74de3ab198cfa9ca19b12 |
| Source note | uspto-grants-2015_11 |