HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 118363874, compound → HCID 71248026, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 118363874 | HCID 118363874 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 71248026 | HCID 71248026 | 68.7% |
Reaction Steps
To a solution of 61 (1.04 g, 2.09 mmol) and EtOH (25 mL), was added Pd/C (10% Degussa wet, 0.5 g). The mixture was hydrogenated overnight under balloon pressure. The mixture was then filtered and evaporated to afford 0.52 g (68.5%) of 63 as thick oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187462B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-ad0b07b062744187820822a95aa32aab |
| Source note | uspto-grants-2015_11 |