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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 715062Generated: October 30, 2026

HCID 118363874, compound → HCID 71248026, compound

https://huagongshe.com/reaction/715062

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 118363874HCID 118363874—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 71248026HCID 7124802668.7%

Reaction Steps

To a solution of 61 (1.04 g, 2.09 mmol) and EtOH (25 mL), was added Pd/C (10% Degussa wet, 0.5 g). The mixture was hydrogenated overnight under balloon pressure. The mixture was then filtered and evaporated to afford 0.52 g (68.5%) of 63 as thick oil.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09187462B2
Source datasetuspto-grants-2015_11
ORD IDord-ad0b07b062744187820822a95aa32aab
Source noteuspto-grants-2015_11