HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl formate → HCID 89875126, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl formate | HCID 74626 | — |
| Reactant | HCID 89874983 | HCID 89874983 | — |
| Product | HCID 89875126 | HCID 89875126 | 64% |
Reaction Steps
The title compound is prepared in 64% yield (130 mg, colorless solid) from 4-chloro-2-((5-methyl-6-(2,2,2-trifluoroethoxy)pyridazin-3-yl)methyl)-2,3-dihydro-1H-pyrrolo[3,4-c]pyridin-1-one (170 mg, 0.46 mmol, Intermediate-67) and phenyl formate (110 mg, 0.91 mmol) in a similar manner to Intermediate-91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187475B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-8d44fcd652274981b9b87ae4d8f55509 |
| Source note | uspto-grants-2015_11 |