HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butylsulfinamide, (S)-(-)- → HCID 89875522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butylsulfinamide, (S)-(-)- | HCID 11355477 | — |
| Reactant | HCID 67510144 | HCID 67510144 | — |
| Product | HCID 89875522 | HCID 89875522 | 83% |
Reaction Steps
The title compound is prepared in 83% yield (0.79 g, colorless oil) from 1-(5-methyl-6-(2,2,2-trifluoroethoxy)pyridin-3-yl)ethanone (0.66 g, 2.81 mmol, Step-3 of Amine-2) and (S)-2-methylpropane-2-sulfinamide in a similar manner to Step-4 of Amine-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187475B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-b5736fc77c24489b9343e602f86250f1 |
| Source note | uspto-grants-2015_11 |