HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butylsulfinamide, (R)-(+)- → HCID 89874474, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butylsulfinamide, (R)-(+)- | HCID 10964479 | — |
| Reactant | HCID 89874679 | HCID 89874679 | — |
| Product | HCID 89874474 | HCID 89874474 | 85% |
Reaction Steps
The title compound is prepared in 85% yield (4.10 g, colorless oil) from 1-(6-(cyclopropylmethoxy)-5-methylpyridin-3-yl)ethanone (3.18 g, 15.5 mmol, Step-3) and (R)-2-methylpropane-2-sulfinamide (2.82 g, 23.3 mmol) in a similar manner to Step-4 of Amine-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187475B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-46f40e2915a24b37a74fa1ffd8975bfd |
| Source note | uspto-grants-2015_11 |