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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 715585Generated: October 31, 2026

HCID 118037353, compound → HCID 20735409, compound

https://huagongshe.com/reaction/715585

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 118037353HCID 118037353—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventEthanolHCID 702—
ProductHCID 20735409HCID 20735409—

Reaction Steps

Benzyl 4-(isopropylcarbamoyloxy)piperidine-1-carboxylate (113 mg) is dissolved in ethanol (3 mL), treated with palladium on carbon (10%, 38 mg) and the mixture is hydrogenated at room temperature for 8 hours under 3 bar hydrogen pressure. Then the catalyst is filtered off and washed with ethanol. The combined mother liquours are concentrated to give the title compound, which is used directly in the next step.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09187477B2
Source datasetuspto-grants-2015_11
ORD IDord-54beba9a5a8a4a26bf7bdacda2fdf46b
Source noteuspto-grants-2015_11