HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → Itaconic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Itaconic acid | HCID 811 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | Itaconic acid | HCID 811 | — |
| Product | Methacrylic Acid | HCID 4093 | — |
| Product | Acrylonitrile | HCID 7855 | — |
Reaction Steps
95 mol % of acrylonitrile, 3 mol % of methacrylic acid and 2 mol % of itaconic acid were polymerized by solution polymerization using dimethylsulfoxide as a solvent, and then ammonia was added thereto in an amount equivalent to that of itaconic acid to neutralize the reaction product to prepare a polyacrylontrile-based copolymer in the form of an ammonium salt, thereby obtaining a spinning solution including 22 wt % of the polyacrylontrile-based copolymer.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187847B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-f7ee1799bfea4315b1ba253a3883535b |
| Source note | uspto-grants-2015_11 |