Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 12-Tricosanol | HCID 3084429 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | 2-Propanol, sodium salt (1:1) | HCID 10920443 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 118516617 | HCID 118516617 | — |
Reaction Steps
3.1 g (0.135 mole) sodium metal was dissolved in 40 ml isopropanol under reflux conditions for 4 hrs to make a solution of sodium isopropanolate in isopropanol. 47 g (0.138 mole) 12-tricosanol was added and the resulting isopropanol was subsequently evaporated by heating to 170-180° C. for 2 hrs to yield the sodium 12-tricosanolate for further reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09193653B1 |
|---|
| Source dataset | uspto-grants-2015_11 |
|---|
| ORD ID | ord-5772d3fcb1294c5889405528cee9b9dc |
|---|
| Source note | uspto-grants-2015_11 |
|---|
