HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatoic Anhydride → N-isoprenyl isatoic anhydride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Bromoisoprene | HCID 53976308 | — |
| Product | N-isoprenyl isatoic anhydride | HCID 131734149 | — |
Reaction Steps
Reagents: Isatoic anhydride (6.13 mmols, 1 g); Sodium hydride (9.2 mmols, 0.23 g); Isoprenyl bromide (12 mmols, 1.9 g). Yield: 0.95 g (67%), white solid, m.p.=119° C.-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193688B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-a156aeb4fb5b461da904b7748364092e |
| Source note | uspto-grants-2015_11 |