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HRID716744

反应详情

EQUATION

反应方程式

HRID 716744 的结构方程式

REACTANTS

反应物

2
结构：CC(C)S(=O)(=O)Cl
HCID82408

Isopropyl sulfonyl chloride

C3H7ClO2S

结构：CC(C)(C)OC(=O)NCCOc1cccc(N)c1
HCID11557882

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)S(=O)(=O)Nc1cccc(OCCNC(=O)OC(C)(C)C)c1
HCID68524470

未命名化合物

PROCEDURE

实验过程

Sulfonation of tert-butyl 2-(3-aminophenoxy)ethylcarbamate (3) using propane-2-sulfonyl chloride following the method described in Example 1 gave tert-butyl 2-(3-(1-methylethylsulfonamido)phenoxy)ethylcarbamate (7) as a light yellow oil. 1H NMR (400 MHz, DMSO-d6) δ 9.70 (s, 1H), 7.17 (t, J=8.0 Hz, 1H), 6.97 (t, J=6.0 Hz, 1H), 6.76-6.79 (m, 2H), 6.60-6.62 (m, 1H), 3.16-3.30 (m, 3H), 1.35 (s, 9H), 1.19 (d, J=6.8 Hz, 6H).