HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pentanal → 3-Hydroxy-3-(3-(pentylamino)phenyl)propanenitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pentanal | HCID 8063 | — |
| Reactant | 3-Hydroxy-3-(3-nitrophenyl)propanenitrile | HCID 59316907 | — |
| Product | 3-Hydroxy-3-(3-(pentylamino)phenyl)propanenitrile | HCID 67296594 | — |
Reaction Steps
Hydrogenation of nitrobenzene 11 (0.8 g, 4.2 mmol) and pentanal (0.45 ml, 4.2 mmol) following method described in Example 11 gave 3-hydroxy-3-(3-(pentylamino)phenyl)propanenitrile as a light yellow oil. Yield (0.90 g, 77%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193669B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-d7299af33ee040cfb96b132c95129a38 |
| Source note | uspto-grants-2015_11 |