HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 90269097, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 71761597 | HCID 71761597 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 90269097 | HCID 90269097 | 68% |
Reaction Steps
0.5 mmol of 4-((3-phenyl-isoxazol-5-yl)-methoxy-)-quinazoline was added in 20 mL mixing solution of 5% hydrochloric acid solution and methanol (V:V=1:1), and dissolved by stirring under slightly heating. The mixture was slowly evaporated and crystallized at room temperature to afford 4-((3-phenyl-isoxazol-5-yl)-methoxy-)-quinazoline hydrochloride as a white solid in 68% yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193718B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-58b53271aa634e619b2382f1f0d4e04a |
| Source note | uspto-grants-2015_11 |