HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Fluorophenylboronic acid → HCID 71284101, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Fluorophenylboronic acid | HCID 2734354 | — |
| Reactant | HCID 71284108 | HCID 71284108 | — |
| Product | HCID 71284101 | HCID 71284101 | — |
Reaction Steps
The title compound was prepared from 8-bromo-4-(pyridazin-4-yl)-1H-benzo[b][1,4]diazepin-2(3H)-one (Example 1; 1 mmol) and commercial available 2-fluorophenylboronic acid (CAS-No: 1993-03-9; 1.5 mmol) according to the general procedure G. Obtained as a yellow solid (67%), MS (EI) 333 [(M+1)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193710B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-10a41ee52c234ca6984407ecb6622d43 |
| Source note | uspto-grants-2015_11 |