HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 66992779, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,4-Dioxane | HCID 31275 | — |
| Reactant | HCID 58515955 | HCID 58515955 | — |
| Product | HCID 66992779 | HCID 66992779 | 199.1% |
Reaction Steps
tert-Butyl 4-(6-acetyl-8-chloroimidazo[1,5-a]pyridin-5-yl)piperazine-1-carboxylate (19 mg, 0.051 mmol) was taken into a vial and 4.0 M hydrogen chloride in 1,4-dioxane (1.0 mL, 4.0 mmol) was added and was stirred for 15 minutes. The solvents were evaporated to give the desired compound (16 mg, quantitative). LCMS calculated for C13H16ClN4O (M+H)+: m/z=279.1. found: 278.9.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193721B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-cb25477e57dc449fa430bff5a9eb21a4 |
| Source note | uspto-grants-2015_11 |