HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 3419205, compound → HCID 20116191, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 3419205 | HCID 3419205 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20116191 | HCID 20116191 | — |
Reaction Steps
N-Isopentyl-4-nitrobenzamide (1 g, 4.23 mmol) and methanol (40 ml) were added to palladium on carbon (0.200 g, 1.879 mmol) in a 250 mL SS pressure bottle and the mixture was stirred for 6 hours with hydrogen at 30 psi and room temperature. The mixture was filtered through a nylon membrane and concentrated to provide the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193723B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-d1d53e772a1b4f40b98c3fa453dd293e |
| Source note | uspto-grants-2015_11 |