Hydrochloric Acid → (1s,4s)-2-Benzhydryl-2,5-diazabicyclo[2.2.1]heptane2hcl

Beteiligte Stoffe

Reaktionsschritte

A solution of compound 200 (0.5 g, 1.37 mmol) in 4N HCl in dioxane (5 mL) was stirred for 1 h at room temperature and then concentrated. The residue was purified by trituration with Et2O and filtered to afford 201 (0.24 g, 59%) as a beige solid. LRMS (ESI): (calc) 264.2. (found) 265.3 (MH)+.

Herkunft & Nachweise