HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid methylene chloride → HCID 131734173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid methylene chloride | HCID 21863450 | — |
| Reactant | HCID 117732499 | HCID 117732499 | — |
| Product | HCID 131734173 | HCID 131734173 | — |
Reaction Steps
A solution of compound 41e (0.50 g, 0.93 mol) in TFA/DCM (1:3, 10 mL) was stirred at rt for 2 h. The resulting mixture was concentrated under reduced pressure to obtain compound 41f as a yellow solid. Mass Spectrum (LCMS, ESI pos.): Calcd. for C26H26N6O: 439.2 (M+H). found: 439.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193736B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-e68f2e602cd7410baca82eba0ca072ef |
| Source note | uspto-grants-2015_11 |