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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 718630Generated: October 30, 2026

Trifluoroacetic acid methylene chloride → HCID 131734173, compound

https://huagongshe.com/reaction/718630

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acid methylene chlorideHCID 21863450—
ReactantHCID 117732499HCID 117732499—
ProductHCID 131734173HCID 131734173—

Reaction Steps

A solution of compound 41e (0.50 g, 0.93 mol) in TFA/DCM (1:3, 10 mL) was stirred at rt for 2 h. The resulting mixture was concentrated under reduced pressure to obtain compound 41f as a yellow solid. Mass Spectrum (LCMS, ESI pos.): Calcd. for C26H26N6O: 439.2 (M+H). found: 439.2.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09193736B2
Source datasetuspto-grants-2015_11
ORD IDord-e68f2e602cd7410baca82eba0ca072ef
Source noteuspto-grants-2015_11