HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylhydrazine → Ethyl 2-(1-methylhydrazinyl)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylhydrazine | HCID 6061 | — |
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Product | Ethyl 2-(1-methylhydrazinyl)acetate | HCID 20288078 | 77.2% |
Reaction Steps
According to the procedure described in the synthesis method of Compound XV-1 with the modification that the reaction was carried out overnight, methylhydrazine 7.13 ml (150 mmol) was reacted with ethyl 2-bromoacetate 16.7 g (100 mmol) to obtain the title compound 10.2 g (77%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193734B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-37bbbc975dcb4789991e119d43875f6e |
| Source note | uspto-grants-2015_11 |