Ethyl Bromide → HCID 21896531, compound

HRID 719078Notes

Reaction equation

HRID 719078 reaction equation
[CH3:1][C:2]([CH3:10])([CH:5]([OH:9])[CH:6]([CH3:8])[CH3:7])[CH2:3][OH:4].[CH2:11](Br)[CH3:12]>>[CH2:11]([O:4][CH2:3][C:2]([CH3:10])([CH3:1])[CH:5]([OH:9])[CH:6]([CH3:8])[CH3:7])[CH3:12]

Participants

3

Reactant 2

HCID 6332Ethyl BromideHCID 89462,2,4-Trimethyl-1,3-pentanediol

Product 1

HCID 21896531HCID 21896531, compoundYield 90%

Procedure

Treatment of 2,2,4-trimethylpentan-1,3-diol with ethyl bromide employing the alkylation reaction conditions described above provided 1-ethoxy-2,2,4-trimethylpentan-3-ol in 90.0% yield (313.2 g, b.p.=79–80 C./3.2 mmHg).

Sources & evidence

ORD record
ord-9965e028ecd8420d9bb32cebd1a8c419
Source dataset
uspto-grants-2006_11
Patent number
US07132391B2

Reaction notes

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