HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21896882, compound → HCID 178467022, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21896882 | HCID 21896882 | — |
| Reactant | HCID 21896899 | HCID 21896899 | — |
| Reactant | 5-(4-chloro-phenyl)-4-cyclopentylmethyl-2-(2-ethoxy-4-methoxy-phenyl)-4,5-dihydro-1H-imidazole | HCID 178467016 | — |
| Product | HCID 178467022 | HCID 178467022 | — |
Reaction Steps
5-(4-Chloro-phenyl)-2-(2-ethoxy-4-methoxy-phenyl)-4-isobutyl-4,5-dihydro-1H-imidazole was prepared from 1-(4-chloro-phenyl)-4-methyl-pentane-1,2-diamine and ethyl 2-ethoxy-4-methoxy-benzimidate hydrochloride in an analogous manner as described for the preparation of 5-(4-chloro-phenyl)-4-cyclopentylmethyl-2-(2-ethoxy-4-methoxy-phenyl)-4,5-dihydro-1H-imidazole (Example 9). HR-MS (ES, m/z) observed 387.1837, calculated for C22H28N2O2Cl [(M+H)+]387.1834.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132421B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-b64601ee56e94635ac5f4560fb35dacd |
| Source note | uspto-grants-2006_11 |