Selenium Dioxide → HCID 12336408, compound

HRID 719168Notes

Reaction equation

HRID 719168 reaction equation
[Cl:1][C:2]1[CH:11]=[CH:10][CH:9]=[C:8]2[C:3]=1[CH2:4][CH2:5][CH2:6][C:7]2=[O:12].[Se](=O)=[O:14]>>[Cl:1][C:2]1[CH:11]=[CH:10][CH:9]=[C:8]2[C:3]=1[CH:4]=[CH:5][C:6](=[O:14])[C:7]2=[O:12]

Participants

3

Reactant 2

HCID 24007Selenium DioxideHCID 122065225-CHLORO-1-TETRALONE

Product 1

HCID 12336408HCID 12336408, compound

Procedure

Treatment of 5-chloro-tetralone with selenium dioxide as described in Reference Example 1A yielded 5-chloro-[1,2]naphthoquinone which was coupled with 2,3-diamino-benzoic acid, diacetate salt, as described in Reference Example 1A to yield the title compound.

Sources & evidence

ORD record
ord-d106eb56aafe48c58c86d8d7b177349d
Source dataset
uspto-grants-2006_11
Patent number
US07132419B2

Reaction notes

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