HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 4-Aza-DL-leucine methyl ester. Hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | 28024-66-0 | HCID 303570 | — |
| Product | 4-Aza-DL-leucine methyl ester. Hydrochloride | HCID 131726045 | — |
Reaction Steps
Methanol (150 mL) was saturated with anhydrous hydrogen chloride gas. To this was added 4-aza-DL-leucine (4.86 g)(commercially available) and the reaction mixture was stirred overnight at room temperature. The solvent was removed in vacuo to yield the title compound (quantitative yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132419B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-b04bf8ddf7dc44999c9f7dba726c733b |
| Source note | uspto-grants-2006_11 |