Hydrochloric Acid → 403712-68-5

HRID 719182Notes

Reaction equation

HRID 719182 reaction equation
[ClH:1].[NH2:2][CH:3]([C:8]([OH:10])=[O:9])[CH2:4][N:5]([CH3:7])[CH3:6].[CH3:11]O>>[ClH:1].[CH3:11][O:9][C:8](=[O:10])[CH:3]([CH2:4][N:5]([CH3:7])[CH3:6])[NH2:2]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 887MethanolHCID 30357028024-66-0

Product 1

HCID 131726045403712-68-5

Procedure

Methanol (150 mL) was saturated with anhydrous hydrogen chloride gas. To this was added 4-aza-DL-leucine (4.86 g)(commercially available) and the reaction mixture was stirred overnight at room temperature. The solvent was removed in vacuo to yield the title compound (quantitative yield).

Workup

  1. customThe solvent was removed in vacuo

Sources & evidence

ORD record
ord-b04bf8ddf7dc44999c9f7dba726c733b
Source dataset
uspto-grants-2006_11
Patent number
US07132419B2

Reaction notes

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