HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 11121568, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 10958632 | HCID 10958632 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 11121568 | HCID 11121568 | — |
Reaction Steps
A mixture of 10-fluoro-4-methoxy-benzo[a]phenazine-11-carboxylic acid methyl ester (IV.5) (100 mg) and 2.0M solution of methylamine in tetrahydrofuran was stirred at room temperature for 18 hours. The solvent was then removed in vacuo to yield the crude desired title compound as an orange solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132419B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-0488378b908e477d9c8339afc97ceda9 |
| Source note | uspto-grants-2006_11 |