HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 69596867, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 11102819 | HCID 11102819 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 69596867 | HCID 69596867 | — |
Reaction Steps
To a solution of [11-(2-dimethylamino-ethylcarbamoyl)-benzo[a]phenazin-4-yloxy]-acetic acid tert-butyl ester (18 mg) in dry dichloromethane (1 mL) was added trifluoroacetic acid (1 mL). After stirring for 4 hours the solvent was removed in vacuo to yield crude product. This was triturated with ether to yield the title compound as a yellow solid (10 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132419B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-fa7e7d7ad8594ce7b90d5774b3d9029a |
| Source note | uspto-grants-2006_11 |