HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178483815, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 10270443 | HCID 10270443 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178483815 | HCID 178483815 | 91.8% |
Reaction Steps
A mixture of 4-cyano-benzo[a]phenazine-11-carboxylic acid (2-dimethylamino-ethyl)-amide (20 mg), potassium carbonate (37 mg) and hydroxylamine hydrochloride (19 mg) was heated to reflux in ethanol (5 mL) for 18 hours. The reaction mixture was filtered, and the filtrate was collected and the solvent removed in vacuo to yield the title compound (20 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132419B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-00231bde6c0f4fc49447f804ae6ecc38 |
| Source note | uspto-grants-2006_11 |