HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → HCID 178483814, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | HCID 178483816 | HCID 178483816 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178483814 | HCID 178483814 | — |
Reaction Steps
3-Hydroxy-benzo[a]phenazine-11-carboxylic acid (2-dimethylamino-ethyl)-amide (26 mg) was sonicated in acetic acid (2 mL) to give a fine suspension. To this was added a 40% solution of dimethylamine in water (3 mL) and a 37% solution of formaldehyde in water (3 mL). The reaction mixture was left stirring for 2 days. The volatiles were then removed in vacuo to yield the title compound (29 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132419B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-022a8e4f364444a4af77b7c076646fcb |
| Source note | uspto-grants-2006_11 |