HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pyridine-2-carbonyl chloride → N-[5-(3,4-Dimethoxyphenyl)-3-methyl-1H-pyrazol-4-yl]pyridine-2-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pyridine-2-carbonyl chloride | HCID 135034 | — |
| Reactant | HCID 178489090 | HCID 178489090 | — |
| Product | N-[5-(3,4-Dimethoxyphenyl)-3-methyl-1H-pyrazol-4-yl]pyridine-2-carboxamide | HCID 178489093 | — |
Reaction Steps
The preparation took place in analogy with Example 15a), starting with 200 mg of 5-(3,4-dimethoxyphenyl)-3-methyl-1H-pyrazol-4-ylamine (44) and 168 mg of pyridine-2-carbonyl chloride*HCl. The following was obtained: 55 C18H18N4O3 (338.37); MS (ESI) 339 (M+H)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132428B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-ccab9572a1c44b8597b9bbba7e441b2b |
| Source note | uspto-grants-2006_11 |