HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178434573, compound → HCID 178434202, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178434573 | HCID 178434573 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178434202 | HCID 178434202 | — |
Reaction Steps
The preparation took place in analogy to Example 33 (B), using 401 mg of 2-chloro-N-(3-methyl-5-phenyl-1H-pyrazol-4-yl)-benzamide. The reaction mixture was diluted with water and extracted with dichloromethane. The organic portion was concentrated under reduced pressure and purified by MPLC (4 g SiO2, dichloromethane/methanol=99/1→50/50) to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132428B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-3662fb9a5fab49abba2cd0e52db6b782 |
| Source note | uspto-grants-2006_11 |