HCID 178425843, compound → HCID 178423932, compound

Participants

Reaction Steps

The preparation took place in analogy to example 33 (B), using 192 mg of 4-methyl-N-(3-methyl-5-phenyl-1H-pyrazol-4-yl)-benzamide, except the reaction mixture was diluted with water and extracted with dichloromethane. The organic portion was concentrated under reduced pressure and purified by MPLC (4 g SiO2, dichloromethane/methanol, gradient=99/1→50/50) to give the title compound.

Provenance & Evidence