HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 178424623, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178425291 | HCID 178425291 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 178424623 | HCID 178424623 | — |
Reaction Steps
The preparation took place in analogy to example 34 (D) using 404 mg of 3-methyl-N-(3-methyl-5-phenyl-1H-pyrazol-4-yl)-benzamide, except 10 ml of phosphorous oxychloride was used and the reaction was stirred for 4 hrs. Trituration of the residue with dichloromethane/methanol (95/5) gave the title compound as an off white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132428B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-cd563462dfaa401987bdb713cd097805 |
| Source note | uspto-grants-2006_11 |