Phosphorus oxychloride → HCID 178434200, compound

Participants

Reaction Steps

The preparation took place in analogy to example 34 (D) using 196 mg of 2-bromo-N-(3-methyl-5-phenyl-1H-pyrazole-4-yl)-benzamide, except 6 ml of phosphorous oxychloride was used and the reaction was stirred for 4 hrs. The residue was triturated with dichloromethane to give the title compound as a white solid.

Provenance & Evidence