HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4,6-Trichlorobenzenesulfonyl chloride → HCID 10275773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4,6-Trichlorobenzenesulfonyl chloride | HCID 521335 | — |
| Reactant | 2-amino-4-(4-fluoro-3-methylphenyl)-1,3-thiazole | HCID 2756433 | — |
| Product | HCID 10275773 | HCID 10275773 | — |
Reaction Steps
The title compound was prepared from 2-amino-4-(4′-fluoro-3′-methyl)phenylthiazole and 2,4,6-trichlorobenzenesulfonyl chloride as described in the synthetic METHOD B to give a white solid (50.9 mg) with purity >90%: MS (pos) m/z 451.0, 453.0, 455.0; HRMS m/z 449.9218 (calc. of monoisotopic mass for C16H10Cl3FN2O2S2 gives 449.9233).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132436B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-4f2f18478908401584320ba2a2eeb3ad |
| Source note | uspto-grants-2006_11 |