HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloro-2-methylbenzenesulfonyl chloride → HCID 10158142, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloro-2-methylbenzenesulfonyl chloride | HCID 522734 | — |
| Reactant | 4-(5-Chlorothiophen-2-yl)-1,3-thiazol-2-amine | HCID 701782 | — |
| Product | HCID 10158142 | HCID 10158142 | — |
Reaction Steps
The title compound was prepared from 4-(5-chloro-2-thienyl)-1,3-thiazol-2-amine and 3-chloro-2-methylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a beige solid (29.9 mg) with purity >90%: MS (pos) m/z 405.0, 407.0; HRMS m/z 403.9278 (calc. of monoisotopic mass for C14H10Cl2N2O2S3 gives 403.9281).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132436B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-f5085ab834bc4c5daefbf744799524ed |
| Source note | uspto-grants-2006_11 |